basic multidimensional gas chromatography

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Basic Multidimensional Gas Chromatography
Author : N.A
Publisher : Academic Press
Release Date : 2020-03-20
ISBN 10 : 0128137460
Pages : 330 pages
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Basic Multidimensional Gas Chromatography is aimed at the next generation of multidimensional gas chromatography users who will require basic training in the fundamentals of both GC and GCxGC. This book fills the current need for an inexpensive, straightforward guidebook to get new users started. It will help new users determine when to add or purchase a multidimensional system and teach them to optimize and maximize the capability of each system. Readers will also learn to select specific modes for each portion of a multidimensional analysis. This ideal resource is a concise, hard-hitting text that provides the facts needed to get users up and running. Provides a comprehensive and fundamental introduction to multidimensional gas chromatography Assists readers in determining when to add or purchase a multidimensional system Explains how a given system can be used to its maximum capacity and how users should choose specific modes for different portions of multidimensional analysis

Basic Gas Chromatography
Author : Harold M. McNair,James M. Miller
Publisher : John Wiley & Sons
Release Date : 2011-09-20
ISBN 10 : 1118211200
Pages : 256 pages
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The New Edition of the Well-Regarded Handbook on GasChromatography Since the publication of the highly successful first edition ofBasic Gas Chromatography, the practice of chromatography hasundergone several notable developments. Basic GasChromatography, Second Edition covers the latest in the field,giving readers the most up-to-date guide available, whilemaintaining the first edition's practical, applied approach to thesubject and its accessibility to a wide range of readers. The text provides comprehensive coverage of basic topics in thefield, such as stationary phases, packed columns and inlets,capillary columns and inlets, detectors, and qualitative andquantitative analysis. At the same time, the coverage also featureskey additions and updated topics including: Gas chromatography-mass spectrometry (GC-MS) Sampling methods Multidimensional gas chromatography Fast gas chromatography Gas chromatography analysis of nonvolatile compounds Inverse gas chromatography and pyrolysis gaschromatography Along with these new and updated topics, the references,resources, and Web sites in Basic Gas Chromatography have beenrevised to reflect the state of the field. Concise and fundamentalin its coverage, Basic Gas Chromatography, Second Editionremains the standard handbook for everyone from undergraduatesstudying analytical chemistry to working industrial chemists.

Basic Gas Chromatography
Author : Harold M. McNair,James M. Miller,Nicholas H. Snow
Publisher : John Wiley & Sons
Release Date : 2019-09-11
ISBN 10 : 1119450756
Pages : 284 pages
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Basic Gas Chromatography, Third Edition provides a brief introduction to GC following the objectives for titles in this series. It should appeal to readers with varying levels of education and emphasizes a practical, applied approach to the subject. : This book provides a quick need-to-know introduction to gas chromatography; still the most widely used instrumental analysis technique, and is intended to assist new users in gaining understanding quickly and as a quick reference for experienced users. The new edition provides updated chapters that reflect changes in technology and methodology, especially sample preparation, detectors and multidimensional chromatography. The book also covers new detectors recently introduced and sample preparation methods that have become much more easily accessible since the previous edition.

Gas Chromatography
Author : Colin Poole
Publisher : Elsevier
Release Date : 2012-07-26
ISBN 10 : 0123855411
Pages : 688 pages
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This title provides comprehensive coverage of modern gas chromatography including theory, instrumentation, columns, and applications addressing the needs of advanced students and professional scientists in industry and government laboratories. Chapters are written by recognized experts on each topic. Each chapter offers a complete picture with respect to its topic so researchers can move straight to the information they need without reading through a lot of background information. Individual chapters written by recognized experts The big picture of gas chromatography from theory, to methods, to selected applications Provides references to other sources in associated areas of study to facilitate research Gives access to core data for practical work, comparison of results and decision making

Advanced Gas Chromatography in Food Analysis
Author : Peter Q Tranchida
Publisher : Royal Society of Chemistry
Release Date : 2019-10-30
ISBN 10 : 1788011279
Pages : 478 pages
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Gas chromatography is widely used in applications involving food analysis. Typical applications pertain to the quantitative and/or qualitative analysis of food composition, natural products, food additives, and flavour and aroma components. Providing an up-to-date look at the significant advances in the technology, this book includes details on novel sample preparation processes; conventional, high-speed multidimensional gas chromatography systems, including preparative instrumentation; gas chromatography–olfactometry principles; and, finally, chemometrics principles and applications in food analysis. Aimed at providing the food researcher or analyst with detailed analytical information related to advanced gas chromatography technologies, this book is suitable for professionals and postgraduate students learning about the technique in the food industry and research.

A Practical Guide to Gas Analysis by Gas Chromatography
Author : John Swinley,Piet de Coning
Publisher : Elsevier
Release Date : 2019-06-28
ISBN 10 : 0128188898
Pages : 440 pages
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A Practical Gas Analysis by Gas Chromatography provides a detailed overview of the most important aspects of gas analysis by gas chromatography (GC) for both the novice and expert. Authors John Swinley and Piet de Coning provide the necessary information on the selection of columns and components, thus allowing the reader to assemble custom gas analysis systems for specific needs. The book brings together a wide range of disparate literature on this technique that will fill a crucial gap for those who perform different types of research, including lab operators, separation scientists, graduate students and academic researchers. This highly practical, up-to-date reference can be consulted in the lab to guide key decisions about proper setup, hardware and software selection, calibration, analysis, and more, allowing researchers to avoid the common pitfalls caused by incorrect infrastructure. Shows, in detail, how valve configurations work, allowing readers to understand the building blocks of extremely complex systems Presents the complete infrastructure for setting up a gas analysis laboratory in a single source Includes a full chapter on practical analytical systems for analyzing various gas mixtures

Multidimensional Gas Chromatography for Chiral Analysis
Author : N.A
Publisher : N.A
Release Date : 2018
ISBN 10 :
Pages : 329 pages
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ABSTRACT: Multidimensional gas chromatography (MDGC) is well-established GC method used for a diverse range of applications. Enantioselective MDGC (enantio-MDGC) has been suggested as the method of preference for the separation of extremely overlapping enantiomers. An extensive number of literatures describe enantio-MDGC of polychlorinated biphenyls, essential oils and flavor and fragrance and amino acids were reported. In this review, the applications of MDGC approaches both, heart cutting GC–GC and comprehensive GC × GC in chiral analysis is presented. Since the application of these techniques in this filed is very broad so it will be divided into sections according to the type of the compounds.

Multidimensional Chromatography
Author : Luigi Mondello,Alastair C. Lewis,Keith D. Bartle
Publisher : John Wiley & Sons
Release Date : 2002-02-15
ISBN 10 : 9780471988694
Pages : 452 pages
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Concentrates on the broad field of multidimensional chromatography and its applications in various areas, including pharmaceutical, industrial, environmental, biological and petroleum. Presents information for using multidimensional chromatography in the analytical laboratory. Contains invaluable information put together from the experience and research activities of the authors including Keith Bartle - a pioneer in multidimensional chromatography. First book to discuss all multidimensional techniques Covers a subject area that is part of the exploding field of hypenated techniques Includes a general introduction to all areas of the subject followed by applications

Practical Gas Chromatography
Author : Katja Dettmer-Wilde,Werner Engewald
Publisher : Springer
Release Date : 2014-11-05
ISBN 10 : 3642546404
Pages : 902 pages
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Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.

Handbook of Essential Oils
Author : K. Husnu Can Baser,Gerhard Buchbauer
Publisher : CRC Press
Release Date : 2009-12-28
ISBN 10 : 9781420063165
Pages : 991 pages
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Egyptian hieroglyphs, Chinese scrolls, and Ayurvedic literature record physicians administering aromatic oils to their patients. Today society looks to science to document health choices and the oils do not disappoint. The growing body of evidence of their efficacy for more than just scenting a room underscores the need for production standards, quality control parameters for raw materials and finished products, and well-defined Good Manufacturing Practices. Edited by two renowned experts, the Handbook of Essential Oils covers all aspects of essential oils from chemistry, pharmacology, and biological activity, to production and trade, to uses and regulation. Bringing together significant research and market profiles, this comprehensive handbook provides a much-needed compilation of information related to the development, use, and marketing of essential oils, including their chemistry and biochemistry. A select group of authoritative experts explores the historical, biological, regulatory, and microbial aspects. This reference also covers sources, production, analysis, storage, and transport of oils as well as aromatherapy, pharmacology, toxicology, and metabolism. It includes discussions of biological activity testing, results of antimicrobial and antioxidant tests, and penetration-enhancing activities useful in drug delivery. New information on essential oils may lead to an increased understanding of their multidimensional uses and better, more ecologically friendly production methods. Reflecting the immense developments in scientific knowledge available on essential oils, this book brings multidisciplinary coverage of essential oils into one all-inclusive resource.

Gas Chromatographic Techniques and Applications
Author : Alan John Handley,E. R. Adlard
Publisher : Taylor & Francis
Release Date : 2001
ISBN 10 : 9780849305146
Pages : 337 pages
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This volume provides an overview of the state of the art in gas chromatography with an emphasis on new technologies. The authors-all drawn from respected industrial and academic laboratories-consider developments in gas chromatographic techniques over the last decade. Application areas are addressed within individual chapters.

Multidimensional Chromatography
Author : Luigi Mondello,Alastair C. Lewis,Keith D. Bartle
Publisher : John Wiley & Sons
Release Date : 2002-02-15
ISBN 10 : 9780471988694
Pages : 452 pages
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Concentrates on the broad field of multidimensional chromatography and its applications in various areas, including pharmaceutical, industrial, environmental, biological and petroleum. Presents information for using multidimensional chromatography in the analytical laboratory. Contains invaluable information put together from the experience and research activities of the authors including Keith Bartle - a pioneer in multidimensional chromatography. First book to discuss all multidimensional techniques Covers a subject area that is part of the exploding field of hypenated techniques Includes a general introduction to all areas of the subject followed by applications

Current Practice of Gas Chromatography-Mass Spectrometry
Author : Wilfried M.A. Niessen
Publisher : CRC Press
Release Date : 2001-04-04
ISBN 10 : 9781420029512
Pages : 528 pages
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This volume details the principles and instrumentation of gas chromatography-mass spectrometry (CG-MS), and outlines industrial, environmental, pharmaceutical, clinical, toxicological, forensic and food-related applications, revealing findings from the laboratories of 40 contributing scientists around the world using GC-MS in practice. It describes upstream and downstream applications of GC-MS in the petroleum industry and identifies chlorinated compounds in the environment with quadrupole ion-trap technology and high-resolution sector instruments.

Multidimensional Analytical Techniques in Environmental Research
Author : Regina Duarte,Armando C. Duarte
Publisher : Elsevier
Release Date : 2020-06-06
ISBN 10 : 0128188979
Pages : 314 pages
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Multidimensional Analytical Techniques in Environmental Research is a comprehensive resource on the many multidimensional analytical strategies to qualitatively and quantitatively assess and map the organic and inorganic pollutants in complex atmospheric, water and soil matrices. During the past two decades, the rapidly-evolving field of analytical instrumentation has produced sophisticated multidimensional tools capable of providing unique and in-depth knowledge on the chemical features of complex mixtures from these different environmental matrices. This book brings together the wealth of information in the current literature, assisting in the decision-making process by covering both the fundamentals and applications of these methodologies. Sections cover the wide variety of multidimensional analytical techniques, including multidimensional solution- and solid-state nuclear magnetic resonance (NMR) spectroscopy, ultrahigh-resolution mass spectrometry (MS), two-dimensional correlation spectroscopy, two-dimensional liquid and gas chromatography and capillary electrophoresis coupled to high-resolution detection techniques, and excitation-emission (EEM) fluorescence spectroscopy assisted by multiway data analysis tools, and the use of synchrotron-radiation-based techniques combined with other spectroscopic approaches to explore and map the speciation of elements. Identifies state-of-the-art multidimensional analytical methods for targeted and untargeted profiling of complex mixtures from different environmental matrices (soil, sediment, water, and air) Assesses the advantages and limitations of the most modern and sophisticated multidimensional analytical methods in environmental research Highlights the current challenges and potential future directions in the application of multidimensional analytical tools to advance the current understanding on the dynamics and fate of environmental pollutants in different environmental matrices

Hyphenations of Capillary Chromatography with Mass Spectrometry
Author : Peter Q. Tranchida,Luigi Mondello
Publisher : Elsevier
Release Date : 2019-12-13
ISBN 10 : 012809639X
Pages : 514 pages
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Hyphenations of Capillary Chromatography with Mass Spectrometry provides comprehensive coverage of capillary chromatography with mass spectrometry—both single and multidimensional approaches. The book examines nearly all capillary chromatography approaches, combined with a variety of MS forms, giving readers a wide and detailed view on current-day analytical strategies and applications. Of particular focus are novel developments in the field of MS, such as the Orbitrap, HR ToF, ToF MS with variable electron-impact energy, fast MS-MS and APGC technology. Junior scientists conducting research on mono-dimensional chromatography-MS fundamental relationships and experienced analytical chemists working in conventional capillary chromatography and classical multidimensional chromatography will find this an ideal application-based reference on the hyphenations of these domains. Combines mass spectrometry with a range of chromatographic approaches Emphasizes the importance of both capillary chromatography and mass spectrometry methods, thus stimulating separation scientists to fully exploit both analytical dimensions Authored by two of the world’s leading analytical chemists who have a total of more than 40 years of experience in research and instruction

Introduction to GC-MS Coupling
Author : Stéphane Bouchonnet
Publisher : CRC Press
Release Date : 2013-02-20
ISBN 10 : 1466572515
Pages : 228 pages
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Although GC-MS (gas chromatography–mass spectrometry) finds applications in fields as diverse as the food processing industry, medicine, pharmacology, and environmental analysis, the few works that are dedicated to this use of mass spectrometry are generally highly complex and theoretical. Emphasizing the practical aspects of GC-MS, without neglecting the fundamental theory, Introduction to GC-MS Coupling addresses both novice and experienced users of this technique. It presents GC-MS in a clear, instructive way and proposes solutions for the difficulties classically encountered by users. The book begins with the core principles of gas chromatography and its specific uses with MS detectors. It discusses generalities of mass spectrometry, including the various types of MS detectors and insight into the vacuum necessary for efficient operation. Chapters cover the types of analyzers used in GC-MS and their functioning principles, with a focus on the commonly used quadrupolar analyzers, as well as the implementation, advantages, and limits of various modes of acquisition in GC-MS. The text also compares performance and limitations of quadrupolar analyzers. The author includes a full chapter on quantification using GC-MS, a topic that can be puzzling for many chemists. Encouraging a critical approach to databases, he compares laboratory-made and commercial mass spectra databases, and describes a database research algorithm. The final chapter examines mass spectra interpretation, covering chemistry concepts such as inductive and mesomeric effects required to understand dissociation pathways, and presents a global strategy for mass spectra interpretation.

Columns for Gas Chromatography
Author : Eugene F. Barry, PhD,Robert L. Grob, PhD
Publisher : John Wiley & Sons
Release Date : 2007-04-27
ISBN 10 : 0470114177
Pages : 336 pages
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Choosing the right column is key in Gas Chromatography Gas Chromatography (GC) is the most widely used method for separating and analyzing a wide variety of organic compounds and gases. There have been many recent advancements in both packed column and capillary column GC. With numerous options and considerations, selecting the right column can be complicated. This resource provides essential guidance for scientists and technicians, including: Methods of choosing both capillary and packed columns Selection of dimensions (column length, I.D., film thickness, etc.) and type of column Guidelines for proper connections of the column to the injector and detector United States Pharmacopeia and National Formulary chromatographic methods ASTM, EPA, NIOSH, and OSHA column selection specifications Information on the advantages of computer assistance in GC and multidimensional GC Comprehensive information on column oven temperature control Columns for Gas Chromatography: Performance and Selection is a hands-on reference for scientists and technicians using GC.

Comprehensive Chromatography in Combination with Mass Spectrometry
Author : Luigi Mondello
Publisher : John Wiley & Sons
Release Date : 2011-08-24
ISBN 10 : 1118003454
Pages : 496 pages
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This book provides a detailed description of various multidimensional chromatographic separation techniques. The editor first provides an introduction to the area and then dives right into the various complex separation techniques. While still not used routinely comprehensive chromatography techniques will help acquaint the readers with the fundamentals and possible benefits of multi-dimensional separations coupled with mass spectrometry. The topics include a wide range of material that will appease all interested in either entering the field of multidimensional chromatography and those looking to gain a better understanding of the topic.

Comprehensive Two Dimensional Gas Chromatography
Author : Lourdes Ramos
Publisher : Elsevier
Release Date : 2009-07-22
ISBN 10 : 9780080932699
Pages : 328 pages
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The book reviews the basic concepts and highlights the most relevant advances and developments that have taken place in the field of comprehensive two dimensional gas chromatography (GC x GC) since its introduction in 1991. The several instrumental and technical approaches assayed and developed during these seventeen years and that have contributed to the development of this powerful separation technique and to its increasing application in many areas is explained and comprehensively illustrated through a number of chapters devoted these specific topics. More specialized aspects of the technique, including theoretical aspects, modelization of the chromatographic process, software developments, and alternative couplings is also covered. Finally, special attention is paid to data treatment, for both qualitative and quantitative analysis. This book will be a practical resource that will explain from basic to specialized concepts of GC x GC and will show the current state-of-the-art and discuss future trends of this technique. Outlines basic concepts and principles of GCxGC technique for non-specialists to apply the technique to their research Provides detailed descriptions of recent technical advances and serves as an instructional guide in latest applications in GCxGC Sets the scene for possible future development and alternative new applications of technique

Analytical Gas Chromatography
Author : Walter Jennings
Publisher : Elsevier
Release Date : 2012-12-02
ISBN 10 : 0323141072
Pages : 270 pages
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Analytical Gas Chromatography is a free-standing introduction to and guide through the rapidly progressing field of analytical gas chromatography. The book is divided into 10 chapters that cover various aspects of analytical gas chromatography, from most advantageous column type to troubleshooting. The opening chapters of the book discuss the advantages of the open tubular column over the packed column. This topic is followed by significant chapters on various variables in the gas chromatographic process, including sample injection, stationary phase, carrier gas, and installation. The effect of changes in these variables on the solution elution order is also considered. A chapter also examines the influence of instrumental design features, such as excessive or unswept volumes in the flow path; suitability of the detection mode; and speed and fidelity of the data-handling equipment. The book also presents selected methods that have been employed to achieve better results for a given gas chromatographic problem. The application areas of gas chromatographic process, including food, flavor, fragrance, petroleum- and chemical-related, environment, biology, and medicine, are also presented. The concluding chapter addresses the basic troubleshooting knowledge and considers other chromatographic problems and methods for their rectification.